A Comparison of Three Different High Pressure Liquid Chromatography Systems for the Determination of Aldehydes and Ketones in Diesel Exhaust

George Edward Creech; R. T. Johnson; James O. Stoffer

doi:10.1093/chromsci/20.2.67

A Comparison of Three Different High Pressure Liquid Chromatography Systems for the Determination of Aldehydes and Ketones in Diesel Exhaust

George Edward Creech
, R. T. Johnson
, James O. Stoffer

Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

A normal-phase Bondapak high performance liquid chromatographic (HPLC) system was compared to two different reversed-phase Bondapak C//1//8 systems for separating and quantifying aldehydes and ketones. In the normal-phase system, isocratic elution with 2-propanol (IPA) and hexane produced the best results. One reversed-phase system consisted of two C//1//8 columns in series. The other reversed-phase system consisted of a single radial compression cartridge (RCC). Both reversed-phase systems employed solvent programming with acetonitrile/water as the mobile phase. Ultraviolet (UV) detection at 340 nm was used in all of the systems.

Original language	American English
Journal	Journal of Chromatographic Science
DOIs	https://doi.org/10.1093/chromsci/20.2.67
State	Published - Jan 1 1982

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Chemistry

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title = "A Comparison of Three Different High Pressure Liquid Chromatography Systems for the Determination of Aldehydes and Ketones in Diesel Exhaust",

abstract = " A normal-phase Bondapak high performance liquid chromatographic (HPLC) system was compared to two different reversed-phase Bondapak C//1//8 systems for separating and quantifying aldehydes and ketones. In the normal-phase system, isocratic elution with 2-propanol (IPA) and hexane produced the best results. One reversed-phase system consisted of two C//1//8 columns in series. The other reversed-phase system consisted of a single radial compression cartridge (RCC). Both reversed-phase systems employed solvent programming with acetonitrile/water as the mobile phase. Ultraviolet (UV) detection at 340 nm was used in all of the systems.",

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year = "1982",

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doi = "10.1093/chromsci/20.2.67",

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AU - Johnson, R. T.

AU - Stoffer, James O.

PY - 1982/1/1

Y1 - 1982/1/1

N2 - A normal-phase Bondapak high performance liquid chromatographic (HPLC) system was compared to two different reversed-phase Bondapak C//1//8 systems for separating and quantifying aldehydes and ketones. In the normal-phase system, isocratic elution with 2-propanol (IPA) and hexane produced the best results. One reversed-phase system consisted of two C//1//8 columns in series. The other reversed-phase system consisted of a single radial compression cartridge (RCC). Both reversed-phase systems employed solvent programming with acetonitrile/water as the mobile phase. Ultraviolet (UV) detection at 340 nm was used in all of the systems.

AB - A normal-phase Bondapak high performance liquid chromatographic (HPLC) system was compared to two different reversed-phase Bondapak C//1//8 systems for separating and quantifying aldehydes and ketones. In the normal-phase system, isocratic elution with 2-propanol (IPA) and hexane produced the best results. One reversed-phase system consisted of two C//1//8 columns in series. The other reversed-phase system consisted of a single radial compression cartridge (RCC). Both reversed-phase systems employed solvent programming with acetonitrile/water as the mobile phase. Ultraviolet (UV) detection at 340 nm was used in all of the systems.

UR - https://scholarsmine.mst.edu/chem_facwork/1506

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JO - Journal of Chromatographic Science

JF - Journal of Chromatographic Science

ER -

A Comparison of Three Different High Pressure Liquid Chromatography Systems for the Determination of Aldehydes and Ketones in Diesel Exhaust

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